http://metabolomics.jp/mediawiki/index.php?action=history&feed=atom&title=LCMS%3AAlbizzae_Cortex LCMS:Albizzae Cortex - Revision history 2026-05-15T14:04:06Z Revision history for this page on the wiki MediaWiki 1.19.1 http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284275&oldid=prev Editor at 07:08, 14 February 2011 2011-02-14T07:08:23Z <p></p> <table class='diff diff-contentalign-left'> <col class='diff-marker' /> <col class='diff-content' /> <col class='diff-marker' /> <col class='diff-content' /> <tr valign='top'> <td colspan='2' style="background-color: white; color:black;">← Older revision</td> <td colspan='2' style="background-color: white; color:black;">Revision as of 07:08, 14 February 2011</td> </tr><tr><td colspan="2" class="diff-lineno">Line 1:</td> <td colspan="2" class="diff-lineno">Line 1:</td></tr> <tr><td colspan="2">&#160;</td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">{{LCMS/Header}}</ins></div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/TIC</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/TIC</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|TICFile=Albizziae LC-MS</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|TICFile=Albizziae LC-MS</div></td></tr> </table> Editor http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284274&oldid=prev Editor: moved Albizzae Cortex LC-MS to LCMS:Albizzae Cortex 2011-02-14T02:20:23Z <p>moved <a href="/wiki/Albizzae_Cortex_LC-MS" class="mw-redirect" title="Albizzae Cortex LC-MS">Albizzae Cortex LC-MS</a> to <a href="/wiki/LCMS:Albizzae_Cortex" title="LCMS:Albizzae Cortex">LCMS:Albizzae Cortex</a></p> <table class='diff diff-contentalign-left'> <tr valign='top'> <td colspan='1' style="background-color: white; color:black;">← Older revision</td> <td colspan='1' style="background-color: white; color:black;">Revision as of 02:20, 14 February 2011</td> </tr></table> Editor http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284273&oldid=prev Adm at 04:25, 10 February 2011 2011-02-10T04:25:25Z <p></p> <table class='diff diff-contentalign-left'> <col class='diff-marker' /> <col class='diff-content' /> <col class='diff-marker' /> <col class='diff-content' /> <tr valign='top'> <td colspan='2' style="background-color: white; color:black;">← Older revision</td> <td colspan='2' style="background-color: white; color:black;">Revision as of 04:25, 10 February 2011</td> </tr><tr><td colspan="2" class="diff-lineno">Line 7:</td> <td colspan="2" class="diff-lineno">Line 7:</td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PColumn&#160; &#160; =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PColumn&#160; &#160; =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PTemperature=40</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PTemperature=40</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">PSolvent A&#160; </del>=5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PSolventA&#160; </ins>=5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">PSolvent B&#160; </del>=acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PSolventB&#160; </ins>=acetonitrile</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PGradient&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PGradient&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PVoltage&#160; &#160; =4.5</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|PVoltage&#160; &#160; =4.5</div></td></tr> <tr><td colspan="2" class="diff-lineno">Line 19:</td> <td colspan="2" class="diff-lineno">Line 19:</td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NColumn&#160; &#160; =Waters Atlantis T3 (2.1 mm x 150 mm)</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NColumn&#160; &#160; =Waters Atlantis T3 (2.1 mm x 150 mm)</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NTemperature=40</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NTemperature=40</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">NSolvent A&#160; </del>=5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NSolventA&#160; </ins>=5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">NSolvent B&#160; </del>=acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NSolventB&#160; </ins>=acetonitrile</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NGradient&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NGradient&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NVoltage&#160; &#160; =-3.5</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>|NVoltage&#160; &#160; =-3.5</div></td></tr> </table> Adm http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284272&oldid=prev Adm at 04:14, 10 February 2011 2011-02-10T04:14:50Z <p></p> <table class='diff diff-contentalign-left'> <col class='diff-marker' /> <col class='diff-content' /> <col class='diff-marker' /> <col class='diff-content' /> <tr valign='top'> <td colspan='2' style="background-color: white; color:black;">← Older revision</td> <td colspan='2' style="background-color: white; color:black;">Revision as of 04:14, 10 February 2011</td> </tr><tr><td colspan="2" class="diff-lineno">Line 4:</td> <td colspan="2" class="diff-lineno">Line 4:</td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/LCMS/Pos</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/LCMS/Pos</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Instrument </del>=Shimadzu LC-IT-TOF MS ESI</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PInstrument </ins>=Shimadzu LC-IT-TOF MS ESI</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Column </del>&#160; &#160; =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PColumn </ins>&#160; &#160; =Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Temperature</del>=40</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PTemperature</ins>=40</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Solvent </del>A&#160; =5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PSolvent </ins>A&#160; =5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Solvent </del>B&#160; =acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PSolvent </ins>B&#160; =acetonitrile</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Gradient </del>&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PGradient </ins>&#160; =10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Voltage </del>&#160; =4.5</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PVoltage </ins>&#160; =4.5</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Capillary </del> =200</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PCapillary </ins> =200</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Gas </del>&#160; &#160; &#160; =1.5</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">PGas </ins>&#160; &#160; &#160; =1.5</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/LCMS/Neg</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>{{CrudeDrug/LCMS/Neg</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Instrument </del>=Shimadzu LC-IT-TOF MS ESI</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NInstrument </ins>=Shimadzu LC-IT-TOF MS ESI</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Column </del>&#160; &#160; =Waters Atlantis T3 (2.1 mm x 150 mm)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NColumn </ins>&#160; &#160; =Waters Atlantis T3 (2.1 mm x 150 mm)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Temperature</del>=40</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NTemperature</ins>=40</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Solvent </del>A&#160; =5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NSolvent </ins>A&#160; =5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Solvent </del>B&#160; =acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NSolvent </ins>B&#160; =acetonitrile</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; 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color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NCapillary </ins> =200</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">Gas </del>&#160; &#160; &#160; =1.5</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">NGas </ins>&#160; &#160; &#160; =1.5</div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td></tr> </table> Adm http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284271&oldid=prev Adm at 04:11, 10 February 2011 2011-02-10T04:11:40Z <p></p> <table class='diff diff-contentalign-left'> <col class='diff-marker' /> <col class='diff-content' /> <col class='diff-marker' /> <col class='diff-content' /> <tr valign='top'> <td colspan='2' style="background-color: white; color:black;">← Older revision</td> <td colspan='2' style="background-color: white; color:black;">Revision as of 04:11, 10 February 2011</td> </tr><tr><td colspan="2" class="diff-lineno">Line 1:</td> <td colspan="2" class="diff-lineno">Line 1:</td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">==</del>TIC=<del class="diffchange diffchange-inline">=</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins class="diffchange diffchange-inline">{{CrudeDrug/</ins>TIC</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">[[Image:</del>Albizziae LC-MS<del class="diffchange diffchange-inline">.jpg|thumb|700px|center|LC-MS TIC of extracts]]</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins class="diffchange diffchange-inline">|TICFile</ins>=Albizziae LC-MS</div></td></tr> <tr><td colspan="2">&#160;</td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins class="diffchange diffchange-inline">}}</ins></div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">==Analytical conditions==</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>{<ins class="diffchange diffchange-inline">{CrudeDrug/LCMS/Pos</ins></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>{<del class="diffchange diffchange-inline">| class=&quot;wikitable&quot; style=&quot;width:80%&quot;</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Instrument <ins class="diffchange diffchange-inline">=</ins>Shimadzu LC-IT-TOF MS ESI</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|- </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Column <ins class="diffchange diffchange-inline">&#160; &#160; =</ins>Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Instrument <del class="diffchange diffchange-inline">|| </del>Shimadzu LC-IT-TOF MS ESI <del class="diffchange diffchange-inline">(Positive ion mode)</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Temperature<ins class="diffchange diffchange-inline">=40</ins></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|- </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Solvent A <ins class="diffchange diffchange-inline"> =</ins>5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Column <del class="diffchange diffchange-inline">|| </del>Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Solvent B <ins class="diffchange diffchange-inline"> =</ins>acetonitrile</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Gradient <ins class="diffchange diffchange-inline">&#160; =</ins>10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Column </del>Temperature<del class="diffchange diffchange-inline">|| 40℃&#160; </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">Voltage&#160; &#160; =</ins>4.5</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Capillary <ins class="diffchange diffchange-inline"> =</ins>200</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Solvent A <del class="diffchange diffchange-inline">|| </del>5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">Gas&#160; &#160; &#160; &#160; =</ins>1.5</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins class="diffchange diffchange-inline">}</ins>}</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Solvent B <del class="diffchange diffchange-inline">|| </del>acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Gradient <del class="diffchange diffchange-inline">|| </del>10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Source voltage ||&#160; </del>4.5 <del class="diffchange diffchange-inline">kV</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Capillary <del class="diffchange diffchange-inline">temperature || </del>200 <del class="diffchange diffchange-inline">°C</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Nebulizer gas || </del>1.5 <del class="diffchange diffchange-inline">l/min</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|</del>}</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td><td class='diff-marker'>&#160;</td><td style="background: #eee; color:black; font-size: smaller;"></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>{<del class="diffchange diffchange-inline">| class=&quot;wikitable&quot; style=&quot;width:80%&quot;</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>{<ins class="diffchange diffchange-inline">{CrudeDrug/LCMS/Neg</ins></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|- </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Instrument <ins class="diffchange diffchange-inline">=</ins>Shimadzu LC-IT-TOF MS ESI</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Instrument <del class="diffchange diffchange-inline">|| </del>Shimadzu LC-IT-TOF MS ESI <del class="diffchange diffchange-inline">(Negative ion mode)</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Column <ins class="diffchange diffchange-inline">&#160; &#160; =</ins>Waters Atlantis T3 (2.1 mm x 150 mm)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|- </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Temperature<ins class="diffchange diffchange-inline">=40</ins></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Column <del class="diffchange diffchange-inline">|| </del>Waters Atlantis T3 (2.1 mm x 150 mm)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Solvent A <ins class="diffchange diffchange-inline"> =</ins>5 mM Ammonium acetate solution</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Solvent B <ins class="diffchange diffchange-inline"> =</ins>acetonitrile</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Column </del>Temperature<del class="diffchange diffchange-inline">|| 40℃&#160; </del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Gradient <ins class="diffchange diffchange-inline">&#160; =</ins>10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">Voltage&#160; &#160; =</ins>-3.5</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Solvent A <del class="diffchange diffchange-inline">|| </del>5 mM Ammonium acetate solution</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Capillary <ins class="diffchange diffchange-inline"> =</ins>200</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|<ins class="diffchange diffchange-inline">Gas&#160; &#160; &#160; &#160; =</ins>1.5</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Solvent B <del class="diffchange diffchange-inline">|| </del>acetonitrile</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>}}</div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Gradient <del class="diffchange diffchange-inline">|| </del>10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|-</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Source voltage || – </del>3.5 <del class="diffchange diffchange-inline">kV</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| Capillary <del class="diffchange diffchange-inline">temperature || </del>200 <del class="diffchange diffchange-inline">°C</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|<del class="diffchange diffchange-inline">-</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">| Nebulizer gas || </del>1.5 <del class="diffchange diffchange-inline">l/min</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">|}</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>&#160;</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>&#160;</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>&#160;</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>&#160;</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">==LC-MS raw data==</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>&#160;</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">===Albizzae Cortex LC-MS===</del></div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> <tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div><del class="diffchange diffchange-inline">{{JCampViewer|Albizziae LC-MS.gz</del>}}</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div></div></td></tr> </table> Adm http://metabolomics.jp/mediawiki/index.php?title=LCMS:Albizzae_Cortex&diff=284270&oldid=prev Toyama: New page: ==TIC== LC-MS TIC of extracts ==Analytical conditions== {| class="wikitable" style="width:80%" |- | Instrument || Shimadzu LC-IT-TOF MS E... 2011-02-08T06:14:23Z <p>New page: ==TIC== <a href="/wiki/File:Albizziae_LC-MS.jpg" title="File:Albizziae LC-MS.jpg">LC-MS TIC of extracts</a> ==Analytical conditions== {| class=&quot;wikitable&quot; style=&quot;width:80%&quot; |- | Instrument || Shimadzu LC-IT-TOF MS E...</p> <p><b>New page</b></p><div>==TIC==<br /> [[Image:Albizziae LC-MS.jpg|thumb|700px|center|LC-MS TIC of extracts]]<br /> <br /> ==Analytical conditions==<br /> {| class=&quot;wikitable&quot; style=&quot;width:80%&quot;<br /> |- <br /> | Instrument || Shimadzu LC-IT-TOF MS ESI (Positive ion mode)<br /> |- <br /> | Column || Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron)<br /> |-<br /> | Column Temperature|| 40℃ <br /> |-<br /> | Solvent A || 5 mM Ammonium acetate solution<br /> |-<br /> | Solvent B || acetonitrile<br /> |-<br /> | Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)<br /> |-<br /> | Source voltage || 4.5 kV<br /> |-<br /> | Capillary temperature || 200 °C<br /> |-<br /> | Nebulizer gas || 1.5 l/min<br /> |}<br /> <br /> {| class=&quot;wikitable&quot; style=&quot;width:80%&quot;<br /> |- <br /> | Instrument || Shimadzu LC-IT-TOF MS ESI (Negative ion mode)<br /> |- <br /> | Column || Waters Atlantis T3 (2.1 mm x 150 mm)<br /> |-<br /> | Column Temperature|| 40℃ <br /> |-<br /> | Solvent A || 5 mM Ammonium acetate solution<br /> |-<br /> | Solvent B || acetonitrile<br /> |-<br /> | Gradient || 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min)<br /> |-<br /> | Source voltage || – 3.5 kV<br /> |-<br /> | Capillary temperature || 200 °C<br /> |-<br /> | Nebulizer gas || 1.5 l/min<br /> |}<br /> <br /> <br /> <br /> <br /> ==LC-MS raw data==<br /> <br /> ===Albizzae Cortex LC-MS===<br /> {{JCampViewer|Albizziae LC-MS.gz}}</div> Toyama