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Licoricesaponin H2 - Revision history
2026-06-28T23:32:06Z
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Toyama: /* Spectroscopic Data */
2010-02-09T03:13:31Z
<p><span dir="auto"><span class="autocomment">Spectroscopic Data</span></span></p>
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<td colspan='2' style="background-color: white; color:black;">Revision as of 03:13, 9 February 2010</td>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>| '''IR''' (KBr)<sup>2</sup>|| 3500-3300 (br), 2920, 1725, 1645, 1386, 1200, 1040 cm<sup>-1</sup></div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>| '''IR''' (KBr)<sup>2</sup>|| 3500-3300 (br), 2920, 1725, 1645, 1386, 1200, 1040 cm<sup>-1</sup></div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|-</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|-</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>| '''<sup>1</sup>H-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 500 MHz)<sup>2</sup>|| 0.87 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.06 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.19 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.20 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.35 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.36 (s, <del class="diffchange diffchange-inline">CH3</del>), 1.38 (s, <del class="diffchange diffchange-inline">CH3</del>), 3.00 (brd, ''J''= 13.0 Hz, H-18), 3.35 (dd, ''J''=4.0. 12.3 Hz, H-3), 4.97 (d, ''J''=7.6 Hz, H-1 of GlcUA I), 5.35 (d, ''J''=7.6 Hz, H-1 of GlcUA II), 5.79 (brs, H-12)</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>| '''<sup>1</sup>H-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 500 MHz)<sup>2</sup>|| 0.87 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.06 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.19 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.20 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.35 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.36 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 1.38 (s, <ins class="diffchange diffchange-inline">CH<sub>3</sub></ins>), 3.00 (brd, ''J''= 13.0 Hz, H-18), 3.35 (dd, ''J''=4.0. 12.3 Hz, H-3), 4.97 (d, ''J''=7.6 Hz, H-1 of GlcUA I), 5.35 (d, ''J''=7.6 Hz, H-1 of GlcUA II), 5.79 (brs, H-12)</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|-</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|-</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>| '''<sup>13</sup>C-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 125MHz)<sup>1</sup>|| 105.0 (C-1 of Glc I), 106.8 (C-1 of Glc II), 128.8 (C-12), 169.0 (C-13), 180.6 (C-29), 199.4 (C-11)</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>| '''<sup>13</sup>C-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 125MHz)<sup>1</sup>|| 105.0 (C-1 of Glc I), 106.8 (C-1 of Glc II), 128.8 (C-12), 169.0 (C-13), 180.6 (C-29), 199.4 (C-11)</div></td></tr>
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Toyama
http://metabolomics.jp/mediawiki/index.php?title=Licoricesaponin_H2&diff=107973&oldid=prev
Toyama at 02:57, 9 February 2010
2010-02-09T02:57:35Z
<p></p>
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<td colspan='2' style="background-color: white; color:black;">Revision as of 02:57, 9 February 2010</td>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|SysName=(<del class="diffchange diffchange-inline">3.beta.</del>,<del class="diffchange diffchange-inline">20.alpha.</del>)-20-<del class="diffchange diffchange-inline">carboxy</del>-11-oxo-30-norolean-12-en-3-yl 2-O-<del class="diffchange diffchange-inline">.</del>beta<del class="diffchange diffchange-inline">.</del>-D-glucopyranuronosyl-<del class="diffchange diffchange-inline">.</del>beta<del class="diffchange diffchange-inline">.</del>-D-<del class="diffchange diffchange-inline">Glucopyranosiduronic </del>acid</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|SysName=(<ins class="diffchange diffchange-inline">3beta</ins>,<ins class="diffchange diffchange-inline">20alpha</ins>)-20-<ins class="diffchange diffchange-inline">Carboxy</ins>-11-oxo-30-norolean-12-en-3-yl 2-O-beta-D-glucopyranuronosyl-beta-D-<ins class="diffchange diffchange-inline">glucopyranosiduronic </ins>acid</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|Common Name=&&Licoricesaponin H2&&30-Noroleanane<del class="diffchange diffchange-inline">, .</del>beta<del class="diffchange diffchange-inline">.</del>-D-glucopyranosiduronic acid deriv.&& Saponin H2 from licorice</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Common Name=&&Licoricesaponin H2&&30-Noroleanane beta-D-glucopyranosiduronic acid deriv.&&Saponin H2 from licorice</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td></tr>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>==Mass Spectral Data==</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>==Mass Spectral Data==</div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">==Spectroscopic Data==</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">{| class="wikitable" style="width:80%"</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">'''Free acid'''</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''M.P.'''<sup>1</sup> || 209 - 210 °C </ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''IR''' (KBr)<sup>2</sup>|| 3500-3300 (br), 2920, 1725, 1645, 1386, 1200, 1040 cm<sup>-1</sup></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''<sup>1</sup>H-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 500 MHz)<sup>2</sup>|| 0.87 (s, CH3), 1.06 (s, CH3), 1.19 (s, CH3), 1.20 (s, CH3), 1.35 (s, CH3), 1.36 (s, CH3), 1.38 (s, CH3), 3.00 (brd, ''J''= 13.0 Hz, H-18), 3.35 (dd, ''J''=4.0. 12.3 Hz, H-3), 4.97 (d, ''J''=7.6 Hz, H-1 of GlcUA I), 5.35 (d, ''J''=7.6 Hz, H-1 of GlcUA II), 5.79 (brs, H-12)</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''<sup>13</sup>C-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 125MHz)<sup>1</sup>|| 105.0 (C-1 of Glc I), 106.8 (C-1 of Glc II), 128.8 (C-12), 169.0 (C-13), 180.6 (C-29), 199.4 (C-11)</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|}</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">{| class="wikitable" style="width:80%"</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">'''Trimethyl ester'''</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''M.P.'''<sup>1</sup> || 169 °C </ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''IR''' (KBr)<sup>1</sup>|| 3362, 1722, 1654 cm<sup>-1</sup></ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''<sup>1</sup>H-NMR''' (C<sub>5</sub>D<sub>5</sub>N)<sup>1</sup>|| 4.95 (d, ''J''=7.3 Hz, H-1 of GlcUA I), 5.33 (d, ''J''=7.7 Hz, H-1 of GlcUA II)</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|-</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">| '''<sup>13</sup>C-NMR''' (C<sub>5</sub>D<sub>5</sub>N, 22.5MHz)<sup>2</sup>|| C-3) 89.2, (11) 199.0, (12) 128.6, (13) 168.4, (18) 44.0, (22) 37.1, (24) 16.2, (29) 178.1, (30) 19.3, '''GlcUA I''' (1) 104.9, (2) 84.3, (3) 76.4, (4) 72.5, (5) 77.3, (6) 170.1, '''GlcUA II''' (1)106.8, (2) 76.6, (3) 77.4, (4) 72.9, (5) 77.6, (6) 170.2  </ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">|}</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"><small>1) M. Yoshikawa et al., Chem.Pharm.Bull., 39, 244 (1991)., 2) M. Yoshikawa et al., Chem.Pharm.Bull., 41, 1337 (1993).</small></ins></div></td></tr>
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Toyama
http://metabolomics.jp/mediawiki/index.php?title=Licoricesaponin_H2&diff=107972&oldid=prev
Toyama at 00:49, 8 December 2009
2009-12-08T00:49:06Z
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<td colspan='2' style="background-color: white; color:black;">Revision as of 00:49, 8 December 2009</td>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>}}</div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;">[[Glycyrrhizae Radix LC-MS]]</ins></div></td></tr>
<tr><td colspan="2"> </td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div><ins style="color: red; font-weight: bold; text-decoration: none;"></ins></div></td></tr>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>==Mass Spectral Data==</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>==Mass Spectral Data==</div></td></tr>
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Toyama
http://metabolomics.jp/mediawiki/index.php?title=Licoricesaponin_H2&diff=107971&oldid=prev
Toyama at 00:19, 8 December 2009
2009-12-08T00:19:09Z
<p></p>
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<td colspan='2' style="background-color: white; color:black;">Revision as of 00:19, 8 December 2009</td>
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<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|Common Name=&&30-Noroleanane, .beta.-D-glucopyranosiduronic acid deriv.<del class="diffchange diffchange-inline">&& Licoricesaponin H2</del>&& Saponin H2 from licorice</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Common Name=<ins class="diffchange diffchange-inline">&&Licoricesaponin H2</ins>&&30-Noroleanane, .beta.-D-glucopyranosiduronic acid deriv.&& Saponin H2 from licorice</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td></tr>
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Toyama
http://metabolomics.jp/mediawiki/index.php?title=Licoricesaponin_H2&diff=107970&oldid=prev
Toyama at 00:17, 8 December 2009
2009-12-08T00:17:00Z
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<td colspan="2" class="diff-lineno">Line 3:</td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>{{Metabolite</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid</div></td></tr>
<tr><td class='diff-marker'>−</td><td style="background: #ffa; color:black; font-size: smaller;"><div>|Common Name=30-Noroleanane, .beta.-D-glucopyranosiduronic acid deriv.&& Licoricesaponin H2&& Saponin H2 from licorice</div></td><td class='diff-marker'>+</td><td style="background: #cfc; color:black; font-size: smaller;"><div>|Common Name=<ins class="diffchange diffchange-inline">&&</ins>30-Noroleanane, .beta.-D-glucopyranosiduronic acid deriv.&& Licoricesaponin H2&& Saponin H2 from licorice</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|CAS=118441-85-3</div></td></tr>
<tr><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td><td class='diff-marker'> </td><td style="background: #eee; color:black; font-size: smaller;"><div>|KNApSAcK=</div></td></tr>
</table>
Toyama
http://metabolomics.jp/mediawiki/index.php?title=Licoricesaponin_H2&diff=107969&oldid=prev
Toyama: New page: {{Hierarchy|{{PAGENAME}}}} {{Metabolite |SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid |Common Na...
2009-12-07T23:58:03Z
<p>New page: {{Hierarchy|{{PAGENAME}}}} {{Metabolite |SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid |Common Na...</p>
<p><b>New page</b></p><div>{{Hierarchy|{{PAGENAME}}}}<br />
<br />
{{Metabolite<br />
|SysName=(3.beta.,20.alpha.)-20-carboxy-11-oxo-30-norolean-12-en-3-yl 2-O-.beta.-D-glucopyranuronosyl-.beta.-D-Glucopyranosiduronic acid<br />
|Common Name=30-Noroleanane, .beta.-D-glucopyranosiduronic acid deriv.&& Licoricesaponin H2&& Saponin H2 from licorice<br />
|CAS=118441-85-3<br />
|KNApSAcK=<br />
}}<br />
<br />
==Mass Spectral Data==</div>
Toyama