LCMS:Glycyrrhizae Radix
From Metabolomics.JP
(Difference between revisions)
| Line 10: | Line 10: | ||
| Solvent B || acetonitrile | | Solvent B || acetonitrile | ||
|- | |- | ||
| − | | Gradient || 5% to 100% Solvent B ( | + | | Gradient || 5% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
|} | |} | ||
[[Image:Glycyrrhizae_Radix_LC2.jpg]] | [[Image:Glycyrrhizae_Radix_LC2.jpg]] | ||
| + | {| class="wikitable" style="width:80%" | ||
| + | |- | ||
| + | | Column || Waters Symmetry C18(2.1 mm x 150 mm) | ||
| + | |- | ||
| + | | Column Temperature|| 40℃ | ||
| + | |- | ||
| + | | Solvent A || 0.1% Formic acid solution | ||
| + | |- | ||
| + | | Solvent B || acetonitrile | ||
| + | |- | ||
| + | | Gradient || 5% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) | ||
| + | |} | ||
Revision as of 17:34, 7 December 2009
| Column | Waters Atlantis T3 (2.1 mm x 150 mm) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 5% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Column | Waters Symmetry C18(2.1 mm x 150 mm) |
| Column Temperature | 40℃ |
| Solvent A | 0.1% Formic acid solution |
| Solvent B | acetonitrile |
| Gradient | 5% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
