LCMS:Yokukansan
From Metabolomics.JP
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| − | + | ;Article Title | |
| − | + | : “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.” | |
| − | + | ;Authors | |
| + | : Yamada et.al | ||
| + | ==TIC== | ||
| + | [[Image:Yokukann1.jpg|thumb|700px|center|LC-MS TIC of extracts]] | ||
| + | [[Image:Yokukann2.jpg|thumb|700px|center|LC-MS TIC of standard compounds]] | ||
| − | == | + | ==Analytical conditions== |
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| − | == | + | ==LC-MS raw data== |
===Yokukansan (Tumura)=== | ===Yokukansan (Tumura)=== | ||
Revision as of 13:33, 6 January 2011
- Article Title
- “Ameliorative effects of Yokukansan on learning and memory deficits in olfactory bulbectomized mice.”
- Authors
- Yamada et.al
Contents |
TIC
Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI (Positive ion mode) |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 micron) |
| Column Temperature | 40℃ |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min) |
| Source voltage | 4.5 kV |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |